{"id":3905,"date":"2020-12-29T20:35:18","date_gmt":"2020-12-29T18:35:18","guid":{"rendered":"http:\/\/journal.phaselis.org\/uncategorized\/pha-0126"},"modified":"2020-12-29T21:34:02","modified_gmt":"2020-12-29T19:34:02","slug":"pha-0126","status":"publish","type":"post","link":"http:\/\/journal.phaselis.org\/en\/2020-en\/pha-0126","title":{"rendered":"B\u00f6r\u00fck\u00e7\u00fc Kurtarma Kaz\u0131s\u0131ndaki Arkeolojik Seramik \u00d6rneklerin Spektroskopik Analizleri"},"content":{"rendered":"

Spectroscopic Analysis of Archaeological Ceramic Samples in B\u00f6r\u00fck\u00e7\u00fc Salvage Excavation<\/span><\/strong><\/em><\/p>\n

\u0130lker I\u015eIK<\/strong>
\n\"\" https:\/\/orcid.org\/0000-0003-4510-6100<\/sub><\/p>\n

\u0130smail TARHAN<\/strong>
\n\"\" https:\/\/orcid.org\/0000-0003-3353-8635<\/sub><\/p>\n

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PHASELIS<\/em> VI (2020) 203-215
\n<\/strong>DOI<\/strong>: 10.18367\/Pha.20013
\nReceived Date<\/strong>: 17.09.2020 | Acceptance Date<\/strong>: 20.12.2020
\nOnline Publication Date<\/strong>: 29.12.2020<\/p>\n

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\u00d6z:<\/strong> Bu \u00e7al\u0131\u015fmada, 2003-2008 y\u0131llar\u0131 aras\u0131nda Mu\u011fla \u0130li Yata\u011fan \u0130l\u00e7esi\u2019ndeki T\u00fcrkiye K\u00f6m\u00fcr \u0130\u015fletmeleri (TK\u0130) dekupaj sahas\u0131nda yer alan B\u00f6r\u00fck\u00e7\u00fc Mevkii kurtarma kaz\u0131lar\u0131ndan \u00e7\u0131kar\u0131lan seramik \u00f6rneklerinin kil yap\u0131s\u0131, \u00fcretim tekni\u011fi ile f\u0131r\u0131nlama s\u0131cakl\u0131klar\u0131n\u0131n ve \u015fartlar\u0131n\u0131n tespiti i\u00e7in ATR-FTIR spektroskopisi tekni\u011fi kullan\u0131lm\u0131\u015ft\u0131r. Bu \u00e7al\u0131\u015fman\u0131n amac\u0131, B\u00f6r\u00fck\u00e7\u00fc b\u00f6lgesinden \u00e7\u0131kar\u0131lan seramik \u00f6rneklerinin mineralojik kompozisyonlar\u0131n\u0131 ve f\u0131r\u0131nlama \u015fartlar\u0131n\u0131 FTIR spektroskopisinin t\u00fcm potansiyelini kullanarak tespit etmektir. Sunulan bu \u00e7al\u0131\u015fma B\u00f6r\u00fck\u00e7\u00fc Mevkii\u2019ne ait seramik \u00f6rneklerinin f\u0131r\u0131nlama \u015fartlar\u0131n\u0131n \u00e7al\u0131\u015f\u0131ld\u0131\u011f\u0131 ilk \u00e7al\u0131\u015fma olma \u00f6zelli\u011fine sahiptir. 10 adet farkl\u0131 seramik \u00f6rne\u011fine ait ATR-FTIR spektrumlar\u0131, 1700-400 cm-1 dalga say\u0131s\u0131 aral\u0131\u011f\u0131nda al\u0131nm\u0131\u015ft\u0131r. 2. derece t\u00fcrev spektrumlar\u0131ndan faydalanarak (2. seviye polinomal derece ve 11. seviye Savitzky-Golay yumu\u015fatma noktas\u0131) B\u00f6r\u00fck\u00e7\u00fc\u2019ye ait t\u00fcm seramik \u00f6rneklerinin mineralojik kompozisyonu ve f\u0131r\u0131nlama s\u0131cakl\u0131klar\u0131 ba\u015far\u0131l\u0131 bir \u015fekilde tespit edilmi\u015ftir. Elde edilen sonu\u00e7lara g\u00f6re; \u00e7al\u0131\u015f\u0131lan seramik numunelerinin \u00e7o\u011fu mika-tipi kilden olu\u015ftu\u011fu ve ba\u015fl\u0131ca muskovit, kuvars, al\u00e7\u0131ta\u015f\u0131 ve meta-smektit ve ayr\u0131ca dikkate de\u011fer miktarda bir f\u0131r\u0131nlama minerali olan diopsit i\u00e7erdi\u011fi tespit edilmi\u015ftir. A\u011f\u0131rl\u0131kl\u0131 olarak tespit edilen muskovit, diopsit ve hematit minerallerinin varl\u0131\u011f\u0131 sebebiyle \u00e7al\u0131\u015f\u0131lan seramik numunelerinin \u00e7o\u011funun 800-950 oC aras\u0131nda y\u00fckseltgen bir hava ortam\u0131nda f\u0131r\u0131nland\u0131\u011f\u0131 tespit edilmi\u015ftir.<\/p>\n

Anahtar s\u00f6zc\u00fckler:<\/strong> Arkeoloji, Seramik, F\u0131r\u0131nlama S\u0131cakl\u0131\u011f\u0131, FTIR, Mineral Karakterizasyonu, Spektroskopi<\/p>\n

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Abstract:\u00a0<\/strong>In this study, ATR-FTIR spectroscopy technique was used for the determination of the production technique and firing temperatures and conditions and clay structure of the ceramic samples unearthed from the B\u00f6r\u00fck\u00e7\u00fc Site, which is located in Turkey Coal Enterprises (TKI) decoupage field in Mugla Province, Yatagan District, excavated from rescue excavations between 2003-2008. The aim of this study is to determine the mineralogical composition and firing conditions of the ceramic samples extracted from the B\u00f6r\u00fck\u00e7\u00fc area by using the full potential of FTIR spectroscopy. This presented study has the feature of being the first study in which the firing conditions of ceramic samples belonging to B\u00f6r\u00fck\u00e7\u00fc Mevkii are studied. ATR-FTIR spectra of 10 different ceramic samples were taken in the wavelength range of 1700-400 cm-1. The mineralogical composition and firing temperatures of all ceramic samples belonging to B\u00f6r\u00fck\u00e7\u00fc were successfully determined by using the 2nd order derivative spectra (2nd level polynomal degree and 11th level Savitzky-Golay smoothing point). According to the results obtained; most of the studied ceramic samples were composed of mica-type clay and contain mainly muscovite, quartz, gypsum and meta-smectite, as well as a considerable amount of diopsite which is a firing mineral. It was determined that most of the ceramic samples studied were fired in an oxidizing air atmosphere between 800-950 oC due to the presence of muscovite, diopsite and hematite minerals.<\/p>\n

Keywords:\u00a0<\/strong>Archeology, Ceramics, Firing Temperature, FTIR, Mineral Characterization, Spectroscopy<\/p>\n

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